4.5 Article

Preparation and Characterization of Microcrystalline Cellulose from Sacred Bali Bamboo as Reinforcing Filler in Seaweed-based Composite Film

期刊

FIBERS AND POLYMERS
卷 19, 期 2, 页码 423-434

出版社

KOREAN FIBER SOC
DOI: 10.1007/s12221-018-7672-7

关键词

Biomass; Microcrystalline cellulose; Crystallinity; Seaweed; Reinforcement

资金

  1. Ministry of Higher Education for the Fundamental Research Grant Scheme-Malaysia's Rising Star Award [FRGS-203/PTEKIND/6711531]

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Microcrystalline cellulose (MCC) isolated from cheap, fast-growing and abundant accessible Sacred Bali bamboo (Schizostachyum brachycladum) was utilized as reinforcement material in the seaweed-based composite film. Isolation of MCC was carried out by using a combination of pulping, bleaching and acid hydrolysis process. This study emphasized on the feasibility of MCC production from Sacred Bali bamboo by studying its properties using X-ray diffraction (XRD), scanning electron microscopy (SEM), fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis (TGA). The commercial-MCC (CMCC) was used as reference material. Results showed that the production yield, moisture content (MC) and fiber length of bamboo-MCC (BMCC) were 83.37 +/- 1.48 %, 4.50 +/- 0.5 %, and 0.47 +/- 0.02 mm, respectively. According to the chemical analysis by FTIR, both lignin and hemicellulose were completely removed from BMCC, and thus, improved the crystallinity (78 %) and thermal stability (approximate to 325 degrees C) of BMCC. This study also revealed that MCC produced from Sacred Bali bamboo demonstrated strong mechanical reinforcement effect in the seaweed-based film. Hence, Sacred Bali bamboo-MCC could be used as reinforcement material in the polymer.

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