期刊
RSC ADVANCES
卷 5, 期 91, 页码 74391-74398出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ra14459k
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资金
- CNRS, University Paris Sud
- La Ligue Contre le Cancer
- ANR [ANR-10-LABX-33]
Chemoselective synthesis of ortho ethynylhydrazones 7 derived from 2-iodoacetophenone via a Sonogashira coupling is reported for the first time. In this challenging transformation, a site-selective coupling in the presence of a hydrazone function was developed. These compounds represent useful intermediates for the synthesis of benzofulvenes through a sequence of palladium-catalyzed cross-coupling and palladium-catalyzed 5-exo-dig cyclization.
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