期刊
FOOD CHEMISTRY
卷 177, 期 -, 页码 397-404出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2015.01.060
关键词
Validation; Method development; Aflatoxin; Mycotoxins; Diacetoxyscirpenol; Cereals; Sorghum
资金
- BOF, Ghent University [01W02008]
An LC-MS/MS method was developed and validated for the detection and quantification of 23 mycotoxins in different varieties of sorghum. The method performance characteristics were as follows: suitable linearity ranges for all 23 mycotoxins with p-value >0.05; limits of detection (1.2-50 mu g/kg), limits of quantification (2.5-100 mu g/kg), repeatability (RSDr, 7-22%), intermediate precision (RSDR, 14-44%) and apparent recovery (0.2-11%, expressed as bias). The method was applied to analyze 10 samples obtained from retail shops in Belgium (n = 8) and Germany (n = 2). Nine of the 10 samples (90%) were positive for the following mycotoxins: aflatoxin B-1 (50 mu g/kg), alternariol monomethyl ether (
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