期刊
FOOD CHEMISTRY
卷 174, 期 -, 页码 380-386出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.foodchem.2014.11.068
关键词
Synthetic food colourants; Ionic liquid; HPLC; Aqueous two-phase
资金
- Fund Project of National Natural Science Foundation of China, China [20875082, 21155001]
- Fund Project of Science and Technology of Jiangsu Marine Resources Development Research Institute, China [JSIMR201309]
- Fund Project of Priority Academic Program Development of Jiangsu Higher Education Institutions, China
A rapid and effective method of aqueous two-phase systems based on ionic liquid microextraction for the simultaneous determination of five synthetic food colourants (tartrazine, sunset yellow, amaranth, ponceau 4R and brilliant blue) in food samples was established. High-performance liquid chromatography coupled with an ultraviolet detector of variable wavelength was used for the determinations. 1-alkyl-3-methylimidazolium bromide was selected as the extraction reagent. The extraction efficiency of the five colourants in the proposed system is influenced by the types of salts, concentrations of salt and [CnMIM]Br, as well as the extracting time. Under the optimal conditions, the extraction efficiencies for these five colourants were above 95%. The phase behaviours of aqueous two-phase system and extraction mechanism were investigated by UV-vis spectroscopy. This method was applied to the analysis of the five colourants in real food samples with the detection limit of 0.051-0.074 ng/mL. Good spiked recoveries from 93.2% to 98.9% were obtained. (C) 2014 Elsevier Ltd. All rights reserved.
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