期刊
CERAMICS INTERNATIONAL
卷 44, 期 1, 页码 505-510出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2017.09.204
关键词
Oscillatory pressure sintering (OPS); Microstructure; Mechanical properties; ZTA composites
资金
- China Postdoctoral Science Foundation [2016M600087]
- National Natural Science Foundation of China [51427802, 51672147]
- National Key Research and Development Program of China [2017YFB0310400]
The influence of sintering temperature on the microstructure and mechanical properties of Al2O3 - 20 wt% ZrO2 composites fabricated by oscillatory pressure sintering (OPS) was investigated by means of X-ray diffraction, scanning electron microscopy, three-point bending test and Vickers indentation. Results were compared to specimens obtained by conventional hot pressing (HP) under a similar sintering schedule. The optimum oscillatory pressure sintering temperature was found to be 1600 degrees C; almost fully dense materials (99.94% of theoretical density) with homogeneous microstructure could be achieved. The highest flexural strength, fracture toughness and hardness of such composites reached 1145 MPa, 5.74 MPa m(1/2) and 19.08 GPa when sintered at 1600 degrees C, respectively. Furthermore, the oscillatory pressure sintering temperature could be decreased by more than 50 degrees C as compared with the HP method, OPS favouring enhanced grain boundary sliding, plastic deformation and diffusion in the sintering process.
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