期刊
FLAVOUR AND FRAGRANCE JOURNAL
卷 30, 期 3, 页码 230-237出版社
WILEY-BLACKWELL
DOI: 10.1002/ffj.3235
关键词
aroma glycosides; flue-cured; tobacco; GC-MS; maturity
资金
- Foundation of China Tobacco Anhui Industrial Co., Ltd [2013106, 2014112]
Glycosidically bound aroma compounds in flue-cured tobacco were estimated by capillary gas chromatography-mass spectrometry (GC-MS). After a fast isolation of extracts obtained by HP-20 solid-phase extraction and methanol elution, glycosides were treated with enzymatic hydrolysis and trifluoroacetylation (TFA) before GC-MS analysis. A totall of 21 bound aglycones, mainly consisting of aliphatic alcohol, aromatic components, C-13-norisoprenoids, sesquiterpenoids and polyphenols, were identified by enzymatic hydrolysis. In addition, with the aid of enzymatic hydrolysis, 14 glucosides, one rutinoside and three vicianosides were identified by TFA derivatization. The three vicianosides were identified for the first time in flue-cured tobacco. The norisoprenoids group made up >40% of the total level of aglycons in ripe tobacco, followed by polyphenol and aromatic derivatives (27 and 19%, respectively). Generally, levels of bound compounds increased significantly and the content of total glycosides increased by 36% with maturation. Among the glycosides detected, 3-oxo--ionol-glucoside was the most sensitive to maturity and increased the maximum degree. Copyright (c) 2015 John Wiley & Sons, Ltd.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据