期刊
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
卷 57, 期 17, 页码 4737-4741出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201800240
关键词
amination; C-H functionalization; cross-coupling; electrochemistry; heterocyles
资金
- National Natural Science Foundation of China [21390402, 21520102003]
- Hubei Province Natural Science Foundation of China [2017CFA010]
Dehydrogenative C-H/N-H cross-coupling serves as one of the most straightforward and atom-economical approaches for C-N bond formation. In this work, an electrochemical reaction protocol has been developed for the oxidative C-H amination of unprotected phenols under undivided electrolytic conditions. Neither metal catalysts nor chemical oxidants are needed to facilitate the dehydrogenation process. A series of triarylamine derivatives could be obtained with good functional-group tolerance. The electrolysis is scalable and can be performed at ambient conditions.
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