期刊
REACTION CHEMISTRY & ENGINEERING
卷 2, 期 5, 页码 646-649出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7re00101k
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资金
- Covestro Deutschland AG
- Sapienza Universita di Roma
- MIUR (Ministero dell'Istruzione, dell'Universita e della Ricerca)
Carboxylation of aliphatic and benzyl diamines with electrochemically activated CO2 led to the synthesis of bis-O-alkyl carbamates in high yields. Reaction conditions, including the geometry of the electrochemical cell, were discussed and optimized. This resulted in a significant reduction of unwanted material associated with the reaction, overcoming the economic and environmental restrictions to its application on large scale.
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