期刊
CATALYSTS
卷 7, 期 11, 页码 -出版社
MDPI
DOI: 10.3390/catal7110351
关键词
amidoalkyl naphthols; benzopyrans; supported ionic liquid; magnetically recoverable catalyst
资金
- Natural Science Foundation of Jiangsu Province (China) [BK20150282]
- Natural Science Foundation of the Higher Education Institutions of Jiangsu Province [17KJD430005]
- Innovation and Entrepreneurship Training Program for Undergraduates in Jiangsu Province [201713985010Y, 201710332051X]
- Priority Academic Program Development (PAPD) of Jiangsu Higher Education Institutions
An efficient and eco-friendly procedure for the synthesis of 1-amidoalkyl-2-naphthol and tetrahydrobenzo[b]pyran derivatives has been developed through a one-pot three-component condensation of aldehydes with 2-naphthol and amides, or with malononitrile and dimedone in the presence of magnetic nanoparticle supported acidic ionic liquid (AIL@MNP) as a novel heterogeneous catalyst under solvent-free conditions. This new procedure offers several advantages such as short reaction time, excellent yields, operational simplicity and without any tedious work-up for catalyst recovery or product purification. Moreover, the catalyst could be simply separated by an external magnet and reused six times without significant loss of catalytic activity.
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