4.3 Article

Relevance of the Physicochemical Properties of Calcined Quail Eggshell (CaO) as a Catalyst for Biodiesel Production

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JOURNAL OF CHEMISTRY
卷 2017, 期 -, 页码 -

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HINDAWI LTD
DOI: 10.1155/2017/5679512

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资金

  1. Fundacao Cearense de Apoio ao Desenvolvimento Cientifico e Tecnologico (FUNCAP)
  2. Conselho Nacional de Desenvolvimento Cientifico e Tecnologico (CNPq)
  3. Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES)
  4. DGU [216/12]
  5. Bioinorganic Laboratory (UFC-Chemical)
  6. X-Rays Laboratory (UFC-Physical)
  7. Polymer Laboratory (LAPOL-UFC-Chemical)
  8. Nucleo de Tecnologia do Estado do Ceara (NUTEC)
  9. Universidad de Malaga (UMA)
  10. Ministerio de Economia y Competitividad Project [CTQ 2012-37925-C03-03]
  11. FEDER funds

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The CaO solid derived from natural quail eggshell was calcined and employed as catalyst to produce biodiesel via transesterification of sunflower oil. The natural quail eggshell was calcined at 900 degrees C for 3 h, in order to modify the calcium carbonate present in its structure in CaO, the activity phase of the catalyst. Both precursor and catalyst were characterized using Hammett indicators method, X-ray fluorescence (XRF), X-ray diffraction (XRD), thermogravimetric analysis (TG/DTG), CO2 temperatureprogrammed desorption (CO2-TPD), X-ray photoelectronic spectroscopy (XPS), Fourier infrared spectroscopy (FTIR), scanning electron microscopy (SEM), N-2 adsorption-desorption at -196 degrees C, and distribution particle size. The maximum biodiesel production was of 99.00 +/- 0.02 wt.% obtained in the following transesterification reaction conditions:X-MR (sunflower oil/methanol molar ratio of 1 : 10.5 mol : mol),X-CAT (catalyst loading of 2 wt.%),X-TIME (reaction time of 2 h), stirring rate of 1000 rpm, and temperature of 60 degrees C.

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