4.7 Article

Synthesis of a lithium-cyclopentadienide complex by addition of LiNTf2 to a zwitterionic fulvalene

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DALTON TRANSACTIONS
卷 46, 期 1, 页码 29-32

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ROYAL SOC CHEMISTRY
DOI: 10.1039/c6dt03355e

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The synthesis of a eta(5)-coordinated LiCp complex by simple addition of a Li-salt in benzene is presented. A strongly zwitterionic fulvalene serves as the Cp-precursor. Evidence for the coordination of Li+ was obtained by the characterisitic Li-7 NMR chemical shifts, variable temperature experiments in solution and by X-ray structure analysis in the solid state.

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