期刊
CHEMICAL COMMUNICATIONS
卷 53, 期 4, 页码 716-719出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cc09304c
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资金
- U.S. Department of Energy, Office of Basic Energy Sciences, Division of Chemical Sciences, Geosciences, and Biosciences
- U.S. Department of Energy [DE-AC02-07CH11358]
A beta-SiH functionalized benzyl anion [C(SiHMe2)(2)Ph](-) is obtained by deprotonation of HC(SiHMe2)(2)Ph with KCH2Ph or by reaction of KOtBu and (Me2HSi)(3)CPh; LnI(3)(THF)(n) and three equivalents of this carbanion combine to provide homoleptic tris(alkyl) lanthanide compounds Ln{C(SiHMe2)(2)Ph}(3) (Ln = La, Ce, Pr, Nd) containing secondary metal-ligand interactions.
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