期刊
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
卷 2016, 期 3, 页码 589-598出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejoc.201501305
关键词
Synthetic methods; Cyclization; Radical reactions; Spiro compounds; Acyl radicals; Acylation
资金
- Ministry of Science and Technology (MOST), Republic of China [102-2113-M-194-001-MY3]
A general and efficient method for the preparation of spiro compounds is described. Various enone-aldehydes were exposed to t-dodecanethiol and AIBN at 75 degrees C in toluene to afford spirocyclic 1,4-diketones in moderate to good yields.
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