期刊
CHEMISTRY LETTERS
卷 46, 期 4, 页码 446-448出版社
CHEMICAL SOC JAPAN
DOI: 10.1246/cl.161117
关键词
Sumanene; Aryne; Cycloaddition
资金
- MEXT [26102002]
- JSPS [26288020]
- Grants-in-Aid for Scientific Research [26102002, 26288020] Funding Source: KAKEN
A sumanene-based aryne sumanyne was generated from o-(trifluoromethylsulfonyloxy) sumanenyl pinacolatoborane with CsF under microwave irradiation. Formation of a sumanyne intermediate was confirmed by a reaction with diene compounds to afford the Diels-Alder adducts, and its structure was determined by single-crystal X-ray structure analysis.
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