期刊
CHEMISTRY OF HETEROCYCLIC COMPOUNDS
卷 53, 期 5, 页码 597-603出版社
SPRINGER
DOI: 10.1007/s10593-017-2097-6
关键词
3-nitro-2-phenyl-2-(trifluoromethyl)-2H-chromenes; 3-nitro-2-(trihalomethyl)-2H-chromenes; sodium azide; 4-(trihalomethyl)-2,4-dihydrochromeno[3,4-d][1,2,3]triazoles; 1,3-dipolar cycloaddition
A method was developed for the synthesis of 4-(trihalomethyl)-2,4-dihydrochromeno[3,4-d][1-3]triazoles, based on the reaction of 3-nitro-2-(trifluoro(trichloro)methyl)- and 3-nitro-2-(trifluoromethyl)-2-phenyl-2H-chromenes with sodium azide in DMSO or DMF in the presence of p-toluenesulfonic acid.
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