期刊
ELECTROANALYSIS
卷 29, 期 7, 页码 1755-1761出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/elan.201700025
关键词
NiFe-layered double hydroxide; Nanosheet; Electrochemistry; Non-enzymatic; Glucose sensor
资金
- National High Technology Research and Development Program of China 863 Plan [2015AA034801]
- NSFC [11544010, 11374359, 11304405]
- Nature Science Foundation of Chongqing [cstc2015jcyjA50035, cstc2015jcyjA1660]
- Fundamental Research Funds for the Central Universities [106112016CDJZR288805, 106112015CDJXY300002]
- Chongqing University [201606150016, 201606150017, 201606150056]
- [SKLMT-KFKT-201419]
- [SKLM-ZZKT-2015 Z16]
As a promising electrode material, Ni-based nanomaterials exhibit a remarkable electrochemical catalytic activity for nonenzymatic glucose sensors. In this paper, Nickel-Iron layered double hydroxide (NiFe-LDH) film electrode with ultrathin nanosheets and porous nanostructures was synthesized directly on Ni foam (NF) by a one-step hydrothermal method. The as-obtained NiFe-LDH electrode was adopted for glucose detection without further treatment. As an integrated binder-free electrode for glucose sensor, the NiFe-LDH/NF hybrid exhibits a superior sensitivity of 3680.2 mu A mM(-1) cm(-2) with a low limit of detection (0.59 mu M, S/N=3) as well as fast response time (<1s). An excellent selectivity from potential interference species such as ascorbic acid, uric acid and Cl- ions and acceptable stability were also achieved. The outstanding performance can be ascribed to the abundant electrochemistry active sites, facilitative diffusion of the electrolyte, high electron transfer rate and reliable stability architecture. Therefore, the NiFe-LDH nanosheets demonstrate potential application in non-enzymatic sensory of glucose.
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