期刊
CATALYSIS COMMUNICATIONS
卷 97, 期 -, 页码 138-145出版社
ELSEVIER
DOI: 10.1016/j.catcom.2017.03.017
关键词
1,8-dioxo-octahydroxanthenes; 1,8-dioxo-decahydroacridines; Sulfated zirconia; Heterogeneous catalyst
资金
- Council of Scientific and Industrial Research, New Delhi (CSIR, India)
- CSIR-India
Sulfated zirconia results to be a very efficient catalyst for the synthesis of 1,8-dioxo-octahydroxanthenes and 1,8-dioxo-decahydroacridines without tedious work-up procedures. While 1,8-dioxo-octahydroxanthenes are prepared from aldehyde and 5,5-dimethyl-1,3-cyclohexenedione (dimedone), 1,8-dioxo-decahydroacridines are prepared from this reactant mixture with amines. This method provides a mild catalytic protocol for the synthesis of functionalized xanthene and acridine derivatives. The catalysts were characterized by XRD, FT-IR, TGA-DSC, SEM-EDAX and surface acidity and showed excellent re-usability up to 6 consecutive cycles.
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