期刊
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
卷 56, 期 35, 页码 10539-10544出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/anie.201704910
关键词
C C bond cleavage; cross-coupling; C(sp(3))P bond formation; 1,3-dicarbonyl compounds; silver
资金
- National NSF of China [21502155]
- Fundamental Research Funds for the Central Universities [SWU114077, XDJK2015C103]
The silver-catalyzed oxidative C(sp(3))-H/P-H cross-coupling of 1,3-dicarbonyl compounds with H-phosphonates, followed by a chemo- and regioselective C(sp(3))-C(CO) bond-cleavage step, provided heavily functionalized beta-ketophosphonates. This novel method based on a readily available reaction system exhibits wide scope, high functional-group tolerance, and exclusive selectivity.
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