期刊
CHEMICAL SCIENCE
卷 8, 期 4, 页码 2616-2620出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6sc04541c
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资金
- FWO
- IWT
- Flemish government through Methusalem
- Belspo [IAP-PAI 7/05]
The one-step dehydration, decarboxylation and hydrogenation of the bio-based and widely available citric acid is presented. This reaction sequence yields methylsuccinic acid with yields of up to 89%. Optimal balances between the reaction rates of the different steps were found by varying the hydrogenation catalyst and the reaction parameters (H-2 pressure, pH, temperature, time and catalyst-to-substrate ratio).
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