期刊
CARBOHYDRATE POLYMERS
卷 174, 期 -, 页码 262-272出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.carbpol.2017.06.070
关键词
Chitin; Chitosan; Illex argentinus pen; Response surface methodology; By-products valorization
资金
- POCTEP Programme, EU [0687_NOVOMAR_1_P]
- LIFE+ Programme, EU [iSEAS LIFE13 ENV/ES/000131]
The present report illustrates the optimisation of the experimental conditions for the chemical and enzymatic production of chitin and chitosan from Illex argentinus pen by-products. Optima conditions for chitin isolation were established at 0.82M NaOH/36.4 degrees C, 57.5 degrees C/pH = 9.29, 59.6 degrees C/pH = 9.30 and 49.6 degrees C/pH = 5.91 for chemical, alcalase, espera se and neutrase deproteinization, respectively. Chitin samples were subsequently deacetylated by alkaline treatment reaching the highest degrees of deacetylation (DD > 93%) at 61.0-63.7% of NaOH and 14.9-16.4h of hydrolysis depending on the type of process previously performed to the squid pens. Molecular weight (as number average molecular weight, Mn) of chitosan produced in the experimental designs ranged from 143 kDa (PDI 2.37) to 339 kDa (PDI 2.38). (C) 2017 Elsevier Ltd. All rights reserved.
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