期刊
TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA
卷 27, 期 3, 页码 578-583出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/S1003-6326(17)60064-5
关键词
synthesis; biotemplate; multiple-pore structure; ceria; catalytic performance
资金
- National Natural Science Foundation of China [21277094, 51478285, 21407111]
- Natural Science Foundation of Jiangsu Province, China [BK20140280, BK20151198]
- Collegiate Natural Science Fund of Jiangsu Province, China [14KJA430004]
- Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD), China
- Jiangsu Collaborative Innovation Center of Technology and Material for Water Treatment, China
- Excellent Innovation Team in Science and Technology of Education Department of Jiangsu Province, China
- Jiangsu Key Laboratory for Environment Functional Materials, China [SJHG1304, SJHG1310, SJHG1404]
A biomorphic CeO2 microtube with multiple-pore structure was fabricated by using the cotton as biotemplate, through cerium nitrate solution infiltration and thermal decomposition. Field emission scanning electron microscope (FESEM), powder X-ray diffraction (XRD), transmission electron microscope (TEM), N-2 adsorption-desorption isotherms, temperature-programmed reduction (TPR) and CO oxidation were used to characterize the samples. The results indicated that the synthesized products were composed of crystallites with grain size about 9 nm and exhibited a fibrous morphology similar to the original template and possessed a specific surface area (BET) of 62.3 m(2)/g. Compared with the conventional CeO2 particles, the synthesized materials showed a superior catalytic activity for CO oxidation. For the synthesized fibrous CeO2, the CO conversion at 320 degrees C was above 90% and a 100% CO conversion was obtained at 410 degrees C.
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