期刊
TETRAHEDRON LETTERS
卷 58, 期 22, 页码 2162-2165出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2017.04.075
关键词
MIDA boronates; Photoredox catalysis; Perfluorohaloalkanes; ATRA
资金
- Warsaw University of Technology
The development of a visible light-mediated atom transfer radical addition (ATRA) of perfluoroalkyl iodides to ethynyl-, vinyl- and allyl-MIDA boronates using the reductive and oxidative quenching of [Ru(bPY)(3)]Cl-2 is described. Using an operationally simple and mild protocol, the corresponding MIDA boronates containing perfluoroalkyl groups were obtained in moderate to high yields. The structures of three products were confirmed by single crystal X-ray diffraction studies. (C) 2017 Elsevier Ltd. All rights reserved.
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