期刊
TETRAHEDRON LETTERS
卷 58, 期 41, 页码 3932-3935出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2017.08.065
关键词
Pummerer rearrangement; Sulfoxide; Bis(p-nitrophenyl) phosphorazidate; Azidation; alpha-Azido sulfide
资金
- JSPS [26450145]
- Professor Y. Uozumi's JST-ACCEL program [JPMJAC1401]
- Grants-in-Aid for Scientific Research [26450145] Funding Source: KAKEN
A novel method for the synthesis of azidomethyl sulfides by Pummerer rearrangement using bis(p-nitrophenyl) phosphorazidate (p-NO(2)DPPA) as an azidation reagent was developed. Various methyl sulfoxides were converted into the corresponding azidomethyl sulfides. Importantly, this reaction enables the preparation of azidomethyl sulfides without the use of toxic or explosive azide sources. (C) 2017 Elsevier Ltd. All rights reserved.
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