期刊
TETRAHEDRON LETTERS
卷 58, 期 40, 页码 3846-3850出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2017.08.059
关键词
Palladium catalyst; Heck reaction; Styrenes; Domino reaction; Perfluoroalkyl iodide
资金
- NSFC [21472174, 21602201, 21602204]
- Zhejiang Natural Science Fund for Distinguished Young Scholars [LR16B020002]
A palladium-catalyzed Heck reaction of in-situ generated benzylic iodides and styrenes has been achieved. The reaction proceeds in a one-pot manner through 1) addition perfluoroalkyl iodides to styrenes to give benzylic iodides, 2) followed by a palladium-catalyzed Heck coupling of the resulting benzylic iodides with the same alkenes in high regio- and stereoselectivity. A variety of perfluoroalkylated alkenes were obtained in moderate to excellent yields. (C) 2017 Elsevier Ltd. All rights reserved.
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