期刊
SYNTHETIC COMMUNICATIONS
卷 47, 期 22, 页码 2103-2108出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2017.1365907
关键词
Asteriscunolides; Horner-Wittig-Emmons; macrolide; racemic synthesis; ring-closing metathesis
资金
- Board of Research in Nuclear Sciences [2013/37C/59/BRNS/2443]
A concise total synthesis of racemic asteriscunolide C in eight steps has been described starting from neopentane diol involving an efficient Yamaguchi esterification using an aldehyde-acid, intramolecular Horner-Wittig-Emmons olefination, and a late stage ring-closing metathesis to construct the strained 11-membered ring with one Z- and two E-double bonds.
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