期刊
SYNLETT
卷 29, 期 2, 页码 169-175出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0036-1588554
关键词
deoxygenation; N-Boc-N'-tosylhydrazine; allylic amination; allylic diazene; carbaborane; mercury; catalytic reaction
资金
- MEXT (Ministry of Education, Culture, Sports, Science, and Technology) of the Japanese Government [23790034]
- Grants-in-Aid for Scientific Research [23790034] Funding Source: KAKEN
A m-C2B10H11HgCl/AgOTf-catalyzed reaction of allyl silyl ethers with N-Boc-N'-tosylhydrazine has been developed. Under mild conditions, the resulting allyl hydrazine products were transformed into naked alkenes in good yield. Furthermore, the used m-C2B10H11HgCl could be recovered quantitatively.
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