期刊
CERAMICS INTERNATIONAL
卷 43, 期 1, 页码 1628-1631出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2016.10.108
关键词
CrB2; Borothermal reduction; Molten salt method
资金
- National Natural Science Foundation of China [51302002]
- Graduate Innovation Foundation of Anhui University of Technology [2015075]
- National Training Program of Innovation and Entrepreneurship for Undergraduates [201610360012]
CrB2 powders were successfully synthesized by the borothermal reduction of Cr2O3 at 800-1000 degrees C under ambient pressure without B in excess. The presence of molten NaCl/KCl salts not only greatly decreased the synthesis temperature without introducing any impurities but also induced a small particle size. The CrB2 powders synthesized at 900 degrees C had the largest specific surface area of 11.09 m(2)/g and the lowest equivalent average particle size of 104 nm, respectively.
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