期刊
RUSSIAN JOURNAL OF GENERAL CHEMISTRY
卷 87, 期 9, 页码 1952-1957出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S1070363217090109
关键词
thiacalix[4]arene; amino derivative; Boc-anhydride; alkylation; acylation
资金
- Russian Foundation for Basic Research [16-33-01055_mol_a, 15-03-02877-a]
- Program for Support of Young Russian Scientists (Russian Federation) [SR-1015.2016-4]
Mono-, di-, and tetrasubstituted derivatives of p-tert-butylthiacalix[4]arene containing tert-butylcarbamate, tert-butylcarbonate, and tert-butyl fragments have been prepared for the first time. Depending on the reaction conditions (reagents ratio, temperature, and the presence of a base), the interaction of the monoamine derivative of p-tert-butylthiacalix[4]arene with di-tert-butyl dicarbonate can lead to the formation of mono-, di-, and tetrasubstituted products.
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