期刊
RUSSIAN JOURNAL OF APPLIED CHEMISTRY
卷 90, 期 8, 页码 1214-1218出版社
PLEIADES PUBLISHING INC
DOI: 10.1134/S1070427217080031
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Powdered nanocrystalline europium orthoferrite was synthesized by the glycine-nitrate combustion method, and specific features of its formation were studied in relation to the redox composition of the starting reaction mixture. The products of glycine-nitrate combustion were characterized by X-ray fluorescence microanalysis, X-ray diffraction analysis, scanning electron microscopy, and helium pycnometry. It was found that, depending on the glycine-nitrate ratio, EuFeO3 nanopowders with average crystallite size of 28 +/- 3 to 46 +/- 5 nm can be obtained. The crystallites form under the given conditions porous micrometer-size agglomerates with developed surface. Their morphology and characteristic size vary with the redox composition of the reaction mixture.
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