Microstructural changes of an undisturbed, reconstituted and compacted high plasticity clay subjected to wetting and drying

The behaviour of soil, and in particular compacted clay fill, can have significant implications on the safe and reliable operation of man-made infrastructure. The mechanical behaviour of soil (e.g. volume change and shear strength) is widely recognised as being associated with the microstructural arrangement (fabric/structure). In the case of high plasticity clays, despite the large amount of research carried out, soil microstructure and its evolution along mechanical and hydraulic paths are still not well understood. This makes incorporation of microstructural analysis difficult in engineering practice and highlights the need for further research. A comprehensive microstructural analysis of Maryland clay, a high plasticity residual soil, based on mercury intrusion porosimetry tests, is presented in this paper. Experimental results obtained from undisturbed, reconstituted and compacted specimens subjected to different hydraulic and mechanical paths are described. As with mechanical investigations, the reconstituted state is proposed to be used routinely as a reference state for comparison of undisturbed and compacted soil. The microstructural evolution of the compacted clay, prepared on the wet side of standard Proctor optimum water content, with an initially high void ratio, is examined along the main drying path. Importantly, a monotonic suction increase from the as-compacted state is shown to have negligible effect on the distribution of macro-pores. However, a new insight is provided based on the evolution of the dominant micro-pore entrance diameter which is shown to reduce with increased suction. This micro-pore entrance diameter is shown to correspond with the theoretical suction back-calculated from a simple capillary tube model, up to a limit. It is observed that, under oedometric conditions, the as-compacted microstructure is erased during saturation (soaking) and resembles the reconstituted microstructure. For this particular material and preparation conditions, it is demonstrated that a bimodal microstructure is not recovered on drying from a saturated state. (C) 2015 Elsevier B.V. All rights reserved.