期刊
ORGANIC LETTERS
卷 19, 期 11, 页码 2873-2876出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b01068
关键词
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资金
- Anna Maria Lundin Travel Grant (Smalands Nation)
- Danish National Research Foundation [DNRF118]
- Villum Foundation
- Danish Council for Independent Research: Technology and Production Sciences
A new synthetic approach for introducing N-capping, groups onto peptides attached to a solid support, Combining aminocarbonylation under mild conditions Wing a palladacycle precatalyst and, solid-phase peptide synthesis is reported. The use of la silacarboxylic acid as an in situ CO-releasing molecule allowed the reaction to be performed single vial. The method also enables versatile substitution of side chains, side-chain to side-chain cyclizations, and selective aryl labeling of modified peptides.
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