期刊
ORGANIC LETTERS
卷 19, 期 14, 页码 3755-3758出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b01598
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A constant-current electrochemical method for reducing catalytic nickel complexes in sp(2)-sp(3) cross-electrophile coupling reactions has been developed. The electrochemical reduction provides reliable nickel catalyst activation and turnover and offers a tunable parameter for reaction optimization, in contrast to more standard activated metal powder reductants. The electrochemical reactions give yields (i.e., 51-86%) and selectivities as high or superior to those using metal powder reductants and provide access to a wider substrate Scope.
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