期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 15, 期 6, 页码 1435-1443出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6ob02671k
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资金
- Science and Engineering Research Board (SERB), Indiac under the Fast Track Scheme [SB/FT/CS-073/2014]
- DST, India [SB/FT/CS-100/2012]
Herein we report a microwave assisted Ru(III)/TBHP-mediated reaction of indoles with tetramethylurea (TMU) synthesizing symmetrical as well as unsymmetrical bis(indolyl)methanes, where TMU acts as a methylenating agent. This is the first report where TMU is used as a methylene source. Moreover, the synthesis of unsymmetrical bis(indolyl) methanes by using a carbon precursor is also reported herein for the first time. Various substituted indoles are used for the reaction. The reaction is high yielding and takes a much shorter time to accomplish compared to the existing methods.
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