期刊
NEW JOURNAL OF CHEMISTRY
卷 41, 期 22, 页码 13504-13509出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7nj02975f
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资金
- Fundamental Research Funds for the Central Universities [HIT. NSRIF. 2015046]
- State Key Lab of Inorganic Synthesis and Preparative Chemistry, Jilin University
- Key Laboratory of Functional Inorganic Material Chemistry (Heilongjiang University), Ministry of Education
MIL-100(Fe) is one of the important metal-organic frameworks due to its fascinating physicochemical properties. Generally, MIL-100(Fe) was synthesized under the conditions of adding HF and solvent. Here, we report that MIL-100(Fe) can be facilely synthesized without the addition of solvent and HF. More importantly, this approach can produce MIL-100(Fe) with a high yield of 93%. Additionally, the obtained MIL-100(Fe) exhibited good catalytic performance in the acetalization of benzaldehyde with methanol. This catalyst can still maintain the initial catalytic activity after five cycles.
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