期刊
MONATSHEFTE FUR CHEMIE
卷 148, 期 8, 页码 1463-1468出版社
SPRINGER WIEN
DOI: 10.1007/s00706-017-1944-6
关键词
Sulfated polyborate; Kindler reaction; Thioamides; Solvent free; Recyclable catalyst
资金
- University Grants Commission, New Delhi, India
A rapid, green, and efficient one-pot, three-component Kindler reaction was developed using a sulfated polyborate catalyst. The method described the reaction of aldehydes, amines/ammonium acetate, and sulfur for the synthesis of thioamides using sulfated polyborate under a solvent free condition at 100 degrees C. The key features of the present protocol are high yields, short reaction time, easy workup, and recyclability of a catalyst which gives economical as well as ecological rewards. The present method also has an ability to tolerate a variety of functional groups.
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