期刊
CHEMICAL COMMUNICATIONS
卷 55, 期 8, 页码 1144-1147出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8cc09190k
关键词
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资金
- National Natural Science Foundation of China [21272177]
- Natural Science Foundation of Zhejiang Province [LR15B020002]
A copper-catalyzed isothiocyanation of amines with sodium bromodifluoroacetate and sulfur in the absence of organophosphine has been established. This approach represents a simple and efficient one-pot synthesis of isothiocyanates, and features excellent functional group tolerance and the use of a cheap, safe and odorless sulfur source. Moreover, this process could directly provide isothiocyanate analogous bioactive molecules, thiocarbonyl-containing pesticides and facile construction of benzoxazole and benzimidazole frames.
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