期刊
出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2017.02.071
关键词
Al-Zn-Mg-Er-Zr alloy; Homogenization; Al-3(Er,Zr) particles; Precipitation behavior; Recrystallization resistance
类别
资金
- National Key Research and Development Program of China [2016YFB0300801, 2016YFB0300804]
- Beijing Municipal Science and Technology Project [Z161100002116004]
- National Natural Science Foundation of China [51671005]
- Beijing Natural Science Foundation [2162006]
- Jiangsu Key Laboratory for Clad Materials [BM2014006]
The effects of homogenization treatments on the precipitation behavior of Al-3(Er,Zr) particles and theirs effects on recrystallization resistance in a new type Al-Zn-Mg-Er-Zr alloy have been investigated. Four different homogenization treatments, conventional one-stage homogenization, double-stage homogenization and ramp heating homogenization are carried out. Compared with that in the conventional one-stage homogenization, a finer particle size, higher number density and volume fraction of Al-3(Er,Zr) particles can be obtained in other three homogenization treatments. In addition, the double-stage homogenization and the ramp heating homogenization can improve the Al-3(Er,Zr) particles distribution and minimize the width of precipitation free zone in the region near the grain boundary, and provide an additional but nonnegligible strengthening effect for the Al-Zn-Mg-Er-Zr alloy. The difference in precipitation behavior of Al-3(Er,Zr) particles lead to different recrystallization resistance. The high recrystallization resistance can be attributed to the larger fv/r ratio of Al-3(Er,Zr) particles, which resulting in a higher Zener drag to effectively resist the recrystallization in Al-Zn-MgEr-Zr alloy during hot deformation and the subsequent thermal processing. Therefore, under the same annealing time, the double-stage homogenized and the ramp heating homogenized samples can achieve a significant lower recrystallized fraction compared with the conventional one-stage homogenized samples.
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