4.6 Article

Synthesis of cyclic gem-dinitro compounds via radical nitration of 1,6-diynes with Fe(NO3)3•9H2O

期刊

ORGANIC & BIOMOLECULAR CHEMISTRY
卷 17, 期 19, 页码 4725-4728

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ROYAL SOC CHEMISTRY
DOI: 10.1039/c9ob00431a

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资金

  1. National Natural Science Foundation (NSF) of China [21572203, 21472140]
  2. NSF of Zhejiang Province [LZ16B020001]

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Cyclic gem-dinitro compounds were obtained via nitration of 1,6-diynes using Fe(NO3)(3)center dot 9H(2)O as the nitrating agent. The reaction proceeds at room temperature using a cheap nitrating agent. A number of gem-dinitro cyclic compounds were obtained in moderate to good yields. The reaction offers an easy and convenient protocol to prepare gem-dinitro compounds, which are not easily obtained via the known procedures.

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