期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 17, 期 19, 页码 4725-4728出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9ob00431a
关键词
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资金
- National Natural Science Foundation (NSF) of China [21572203, 21472140]
- NSF of Zhejiang Province [LZ16B020001]
Cyclic gem-dinitro compounds were obtained via nitration of 1,6-diynes using Fe(NO3)(3)center dot 9H(2)O as the nitrating agent. The reaction proceeds at room temperature using a cheap nitrating agent. A number of gem-dinitro cyclic compounds were obtained in moderate to good yields. The reaction offers an easy and convenient protocol to prepare gem-dinitro compounds, which are not easily obtained via the known procedures.
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