期刊
ORGANIC & BIOMOLECULAR CHEMISTRY
卷 17, 期 20, 页码 4979-4983出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9ob00625g
关键词
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资金
- National Natural Science Foundation of China [21502161, 21602187]
- Collaborative Innovation Center of New Chemical Technologies for Environmental Benignity and Efficient Resource Utilization, Scientific Research Fund of Education Department of Hunan Province [16B251]
- Hunan Provincial Natural Science Foundation of China [2017JJ3299]
A concise aerobic photocatalysis using a blue LED combined with a Lewis acid has been developed to enable alpha-thiolation/annulation of carbonyls. Inexpensive, nontoxic Rose Bengal was demonstrated as the best catalyst. Hence, this transition-metal-free protocol allows mild Csp(3)-S couplings with both ketones and aliphatic aldehydes with a range of compatible useful functionalities.
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