期刊
ORGANIC CHEMISTRY FRONTIERS
卷 6, 期 12, 页码 1967-1971出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9qo00358d
关键词
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资金
- National Natural Science Foundation of China [21761006, 21861008]
- Guangxi Natural Science Foundation [2018GXNSFBA138037]
- BAGUI Scholar program of Guangxi province of China
- Central South Unversity
A new electrophilic selenocyanation reagent, selenocyano-benziodoxolone, was successfully prepared from 2-iodobenzoic acid in two steps (71% overall yield). A variety of alpha-selenocyanated ketones and beta-ketoesters, including selenocyanate-containing steroid derivatives, have been achieved by using this newly developed selenocyano-benziodoxolone in good to excellent yields (up to 99%) simply by grinding under mild conditions.
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