期刊
JOURNAL OF SUPERCRITICAL FLUIDS
卷 128, 期 -, 页码 66-72出版社
ELSEVIER SCIENCE BV
DOI: 10.1016/j.supflu.2017.05.006
关键词
Supercritical carbon dioxide; Pyrethrum extract; Pyrethrin; Solubility; Supercritical solvent impregnation; Tick repellent activity
资金
- Ministry of Education, Science and Technological Development of the Republic of Serbia [III45017, ON173006]
This study discusses a possibility of cotton fabric impregnation with pyrethrum extract as a tick repellent in supercritical carbon dioxide. A solubility of pyrethrum extract in supercritical carbon dioxide has been determined at 35 and 40 degrees C and pressures ranging from 8 to 20 MPa. The highest solubility of 48.69 kg/m(3) was obtained at temperature of 35 degrees C and pressure of 20 MPa. Density -based equations of Chrastil, Adachi-Lu and del Valle-Aguilera were employed to correlate the experimental data. Based on the solubility data, conditions for the impregnation of cotton fabric were selected. Conditions at 40 degrees C and 8 MPa provided targeted quantities of the impregnated extract of 0.5% and 1% after 1 h and 2 h of the impregnation, respectively. The presence of pyrethrins on the cotton fabric's surface was confirmed by FTIR analysis. Repellent activity of both impregnated cotton fabrics (pyrethrum extract contents of 0.5% and 1%) was proven against ticks.
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