期刊
JOURNAL OF SEPARATION SCIENCE
卷 40, 期 6, 页码 1266-1272出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201601121
关键词
endocrine-disrupting pesticides; fish; mass spectrometry; pass-through cleanup approach
资金
- Zhejiang Medical Technology and Education Project [2014KYA188]
- Hangzhou Health Science and Technology Major Project [2014z14]
We describe a new methodology for the simultaneous determination of the endocrine-disrupting herbicides (acetochlor, alachlor, amitrole, and atrazine), fungicides (carbendazim, triadimefon, penconazole, and propiconazole), and insecticides (carbaryl and carbofuran) in fish samples followed by high-performance liquid chromatography with tandem mass spectrometry. Samples were extracted and purified using the pass-through cleanup approach. The recoveries of the pesticides were in the range 71.8-116.5%, with relative standard deviations lower than 15.28%. Limits of quantitation were in the range of 0.03-2.50 mu g/kg. Validation results on linearity, accuracy, and precision, as well as on application to the analysis of the endocrine-disrupting pesticides in 20 fish samples, demonstrated the applicability to screen the presence of pesticides in fish.
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