期刊
GREEN CHEMISTRY
卷 21, 期 17, 页码 4706-4711出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9gc02131k
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资金
- National Key Research and Development Program of China [2016YFB0301501]
- National Science Foundation of China [21776130, 21878145]
- Jiangsu Synergetic Innovation Center for Advanced Bio-Manufacture [X1821, X1802]
- Postgraduate Research & Practice Innovation Program of Jiangsu Province
A direct electrochemical oxidative cyclization of alkynoates and alkynamides with diselenides or disulfides for the synthesis of coumarins and quinolinones bearing a chalcogen functional group has been developed. This green and efficient approach was realized through a constant current electrolysis in an undivided cell under metal-free and oxidant-free conditions. Moreover, a series of selenium/sulfur-substituted coumarin and quinolinone products were obtained in moderate to good yields with a broad scope and functional group tolerance.
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