期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 82, 期 13, 页码 6857-6864出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b00994
关键词
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资金
- National Natural Science Foundation of China [21302109, 21302110, 21375075, 21675099]
- Taishan Scholar Foundation of Shandong Province
- Natural Science Foundation of Shandong Province [ZR2015JL004, ZR2016JL012]
- International Cooperation Project of Qinghai Province [2017-HZ-806]
A facile I2O5-mediated direct oxidative coupling of aromatic alkenes with thiols toward vinyl sulfones has been developed under metal-free conditions. This methodology provides a convenient and efficient approach to various (E)-vinyl sulfones from readily available starting materials with excellent regioselectivity. The present oxidative coupling reaction, not only expands the scope of functionalization of alkenes with thiols, but also makes it a practical and powerful complement to traditional methods for the synthesis of (E)-vinyl sulfones.
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