期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 82, 期 18, 页码 9525-9536出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b01547
关键词
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资金
- IISc, SERB, New Delhi [SB/S1/OC-56/2013]
- RL Fine Chem
- CSIR
- IISc
A successful synthesis of alpha-fluoro-beta-ketosulfides using an electrophilic fluorination method has been reported for the first time. The reaction proceeds via an electrophilic fluorination of alpha-sulfenyl-beta-diketones followed by an unexpected tandem deacylation. The resulting products, alpha-fluoro-beta-ketosulfides, are easily oxidized to the corresponding alpha-fluoro-beta-ketosulfones, which can be used for further useful olefination reactions.
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