期刊
GREEN CHEMISTRY
卷 21, 期 23, 页码 6241-6245出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9gc03045j
关键词
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资金
- National Natural Science Foundation of China [21861006]
- Guangxi Natural Science Foundation of China [2016GXNSFEA380001]
- State Key Laboratory for Chemistry and Molecular Engineering of Medicinal Resources [CMEMR2017-A02, CMEMR2017-A07]
A photocatalyst-free visible-light-promoted sulfenylation of quinoxalinones with thiols via cross-dehydrogenative coupling was developed. This protocol allowed the direct formation of diverse 3-sulfenylquinoxalin-2(1H)-ones under metal- and catalyst-free conditions and using air (O-2) as an oxidant. Furthermore, a range of readily accessible thiols and quinoxalin-2(1H)-ones was applied in this coupling, resulting in an attractive process of accessing 3-substituted quinoxalinones.
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