期刊
CHINESE JOURNAL OF ORGANIC CHEMISTRY
卷 39, 期 11, 页码 3176-3182出版社
SCIENCE PRESS
DOI: 10.6023/cjoc201905017
关键词
palladium catalysis; azoxybenzene; acylation; green chemistry
资金
- Key Scientific Research Project for Colleges and Universities of Henan Province [20A150019]
- Doctoral Research Startup Fund of Henan University of Animal Husbandry and Economy [53000168]
A facile and efficient protocol for palladium-catalyzed ortho-acylation of azoxybenzenes has been developed under aqueous conditions. In this process, the alcohols were oxidized into the corresponding aldehydes in situ, which coupled with azoxybenzenes with excellent regioselectivity, affording the acylated azoxybenzenes in moderate to good yields. A variety of functional groups were tolerated in this procedure.
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