期刊
GREEN CHEMISTRY
卷 22, 期 2, 页码 465-470出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9gc03562a
关键词
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资金
- Ministry of Science and Technology of the People's Republic of China [2016YFA0602900]
- National Natural Science Foundation of China [21971072, 21672072, 21420102003]
- Fundamental Research Funds for the Central Universities [2018ZD16]
- Pearl River S&T Nova Program of Guangzhou [201906010072]
- Guangdong Provincial Training Program of Innovation and Entrepreneurship for Undergraduates [S201910561219]
- Hundred Steps Climbing Plan of South China University of Technology [j2tw201902478]
A palladium-catalyzed oxidative aminocarbonylation of O-methyloximes and amines under aerobic conditions with PEG-400 as an environmentally benign medium was accomplished. This novel protocol provides the first straightforward synthetic method for the assembly of structurally diverse 4-carboxamide isoxazoles with high atom- and step-economy and exceptional functional group tolerance. Notably, the employment of ionic liquids as an additive, with air as the sole oxidant, without ligands is an attractive feature of the present approach.
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