期刊
CHEMICAL PAPERS
卷 74, 期 2, 页码 441-449出版社
SPRINGER INTERNATIONAL PUBLISHING AG
DOI: 10.1007/s11696-019-00885-9
关键词
Nitrite; Electrochemical sensor; Au nanoparticles; MoS2 nanosheets; Application
资金
- Natural Science Foundation Committee of Shandong Province, China [ZR2017MB062, BS2013HZ027, ZR2015BL014]
- National Natural Science Foundation of China [21105023]
An electrochemical sensor for the determination of nitrite was successfully fabricated via electro-depositing Au nanoparticles on a glassy carbon electrode (GCE) modified with MoS2 nanosheets. The morphology and composite of the resulted electrode were characterized by scanning electron microscopy ( SEM) and energy dispersive spectroscopy (EDS), respectively. The modified processes of the nanoAu-MoS2/GCE were monitored by cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS). The amperometric current-time (i-t) showed that the developed electrode had excellent response for sodium nitrite under the optimum conditions, and the oxidative current of sodium nitrite was proportionally correlated with its concentration (10-2100 mu M) with a limit of detection (LOD) of 0.09 mu M (S/N = 3), which can be employed in the determination of nitrite in river and drinking water with the advantages of good reproducibility, anti-interference, long-term stability and satisfactory recovery rate.
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