期刊
DALTON TRANSACTIONS
卷 44, 期 39, 页码 16982-17006出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5dt01268f
关键词
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资金
- U.S. National Science Foundation [CHE-1102637]
- Office of Basic Energy Science of the U.S. Department of Energy as part of the Materials Science of Actinides Energy Frontier Research Center [DE-SC0001089]
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1102637] Funding Source: National Science Foundation
This Perspective article highlights some of the traditional and non-traditional analytical tools that are presently used to characterize aqueous inorganic nanoscale clusters and polyoxometalate ions. The techniques discussed in this article include nuclear magnetic resonance spectroscopy (NMR), small angle X-ray scattering (SAXS), dynamic and phase analysis light scattering (DLS and PALS), Raman spectroscopy, and quantum mechanical computations (QMC). For each method we briefly describe how it functions and illustrate how these techniques are used to study cluster species in the solid state and in solution through several representative case studies. In addition to highlighting the utility of these techniques, we also discuss limitations of each approach and measures that can be applied to circumvent such limits as it pertains to aqueous inorganic cluster characterization.
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